Summary
Type: SPE
Application #: 305450
Catalog#: 730950 - SPE Cartridges, Chromabond, HR-XA, 3 ml, 60 mg
Detection:
Conditions: Automated SPE with Gilson GX-271 ASPEC system with single syringe pump type 406 and Trilution LH software version 2.0
Condition 1: 1 mL methanol, 0.5 mL/min
Condition 2: 1 mL ammonia, w(NH3) = 5 %, 0.5 mL/min
Dispense 1: 4 mL sample, 5 mL/min
Dispense 2: 400 µL ammonia, w(NH3) = 26 %, 0.5 mL/min
Load: 1.1 mL mix, 0.5 mL/min
Wash 1: 1 mL ammonia, w(NH3) = 5 %, 0.5 mL/min
Wash 2: 1 mL methanol, 0.5 mL/min
Dry: 5 mL air, 3 mL/min
Elute: 2 x 600 µL hydrochloric acid, c(HCl) = 0.1 mol/L, 0.5 mL/min
Authors: SPE department
Source: Macherey-Nagel, Germany 2010